method development

A board to discuss future MS therapies in early stage (Phase I or II) trials.
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Bobo
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Joined: Tue Aug 24, 2010 2:00 pm

method development

Post by Bobo »

Hi everyone
I am looking for a method for the drug rapamycin,I am currently experiencing fronting. Mobile phase:MeOH\H2O dissolving in MeCN tried flow rates 0.5-1ml/min also tried using buffer with no success.any ideas on what I can do to move foward?
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